Effect of spark plasma sintering temperature on the pore characteristics, porosity and compression strength of porous titanium foams.
Makena, Isaac M. Shongwe, Mxolisi B. Machaka, Ronald Masete, Mosimanegape S.
Makena, Isaac M.
Shongwe, Mxolisi B.
Machaka, Ronald
Masete, Mosimanegape S.
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Abstract
In this work, porous titanium (Ti) foams were successfully produced using spark plasma sintering technique at four different temperatures (up to 650 °C), in conjunction with vacuum sintering (used as a post-treatment) at a constant
temperature of 1200 °C. To obtain a porous structure, 60 vol% of sodium chloride was included as a pore spacer, with the addition of polyethylene glycol solution for Ti–NaCl interparticle binding. The work aimed at studying the effect of
sintering temperature on the final pore features and compression resistance of the porous titanium foams. X-ray diffraction and scanning electron microscopy as characterization techniques were used to analyze phases and pore evolutions,
respectively. The results showed that the pore characteristics and the final porosity of porous titanium foams profoundly depend on the sintering temperature. The lowest porosity of approximately 53.9 vol%, with denser pore walls, was seen at the highest sintering temperature. Such foams sintered at 650 °C can resist the compression stress as high as 123 MPa while exhibiting the stiffness value of 8.1 GPa. The results indicate that the porous Ti foams produced have great potential
for applications in hard tissue engineering.
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Date
2020-02-12
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Publisher
MDPI
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Keywords
Spark plasma sintering, Vacuum sintering, Pore characteristics, Compression test